Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues

Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues

Author: A.R. Fernandez Alba

Publisher: Elsevier

Published: 2004-12-11

Total Pages: 510

ISBN-13: 0080454402

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The trace determination of pesticides continues to be a topic for analytical chemists working in research centres, government and universities. With four chapters devoted to chromatography-mass spectrometry methods, readers are able to understand the analytical basis, technical characteristics and possibilities to evaluate pesticides in food by gas chromatography (GC) and liquid chromatography (LC) mass spectrometry. The book also provides a well-defined and critical compilation of the sample treatment and clean-up procedures, as well as injection techniques applied in GC and LC food analysis. Finally the book deals with aspects related to analytical quality control requirements for pesticide residues, in addition to pesticide regulation aspects. * Contains specific chapters devoted to chromatography-mass spectrometry methods * Provides a well-defined and critical compilation of the sample treatment and clean-up procedures * Contains aspects related to analytical quality control requirements for pesticide residues


Book Synopsis Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues by : A.R. Fernandez Alba

Download or read book Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues written by A.R. Fernandez Alba and published by Elsevier. This book was released on 2004-12-11 with total page 510 pages. Available in PDF, EPUB and Kindle. Book excerpt: The trace determination of pesticides continues to be a topic for analytical chemists working in research centres, government and universities. With four chapters devoted to chromatography-mass spectrometry methods, readers are able to understand the analytical basis, technical characteristics and possibilities to evaluate pesticides in food by gas chromatography (GC) and liquid chromatography (LC) mass spectrometry. The book also provides a well-defined and critical compilation of the sample treatment and clean-up procedures, as well as injection techniques applied in GC and LC food analysis. Finally the book deals with aspects related to analytical quality control requirements for pesticide residues, in addition to pesticide regulation aspects. * Contains specific chapters devoted to chromatography-mass spectrometry methods * Provides a well-defined and critical compilation of the sample treatment and clean-up procedures * Contains aspects related to analytical quality control requirements for pesticide residues


Multiresidue Methods for the Analysis of Pesticide Residues in Food

Multiresidue Methods for the Analysis of Pesticide Residues in Food

Author: Horacio Heinzen

Publisher: CRC Press

Published: 2017-10-10

Total Pages: 531

ISBN-13: 1351644637

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In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.


Book Synopsis Multiresidue Methods for the Analysis of Pesticide Residues in Food by : Horacio Heinzen

Download or read book Multiresidue Methods for the Analysis of Pesticide Residues in Food written by Horacio Heinzen and published by CRC Press. This book was released on 2017-10-10 with total page 531 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.


Analysis of Pesticide Residues

Analysis of Pesticide Residues

Author: H. Anson Moye

Publisher: John Wiley & Sons

Published: 1981-02-02

Total Pages: 488

ISBN-13:

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A comprehensive guide to the latest techniques and applications of pesticide trace analysis. Methods covered include gas, thin layer, and high-performance liquid chromatography, along with their applications in the analysis of chlorinated hydrocarbons, acidic herbicides, organophosphates, carbamates, and insect pheromones and hormones. Includes a special chapter on residue data requirements of government agencies.


Book Synopsis Analysis of Pesticide Residues by : H. Anson Moye

Download or read book Analysis of Pesticide Residues written by H. Anson Moye and published by John Wiley & Sons. This book was released on 1981-02-02 with total page 488 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive guide to the latest techniques and applications of pesticide trace analysis. Methods covered include gas, thin layer, and high-performance liquid chromatography, along with their applications in the analysis of chlorinated hydrocarbons, acidic herbicides, organophosphates, carbamates, and insect pheromones and hormones. Includes a special chapter on residue data requirements of government agencies.


Food Analysis. Determination of Pesticide Residues by LC-MS/MS. Tandem Mass Spectrometric Parameters

Food Analysis. Determination of Pesticide Residues by LC-MS/MS. Tandem Mass Spectrometric Parameters

Author: British Standards Institute Staff

Publisher:

Published: 2007-09-28

Total Pages: 26

ISBN-13: 9780580583537

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Food products, Agricultural products, Plant products, Food testing, Chemical analysis and testing, Determination of content, Residues (pesticides), Pesticides, Liquid chromatography, Mass spectrometry


Book Synopsis Food Analysis. Determination of Pesticide Residues by LC-MS/MS. Tandem Mass Spectrometric Parameters by : British Standards Institute Staff

Download or read book Food Analysis. Determination of Pesticide Residues by LC-MS/MS. Tandem Mass Spectrometric Parameters written by British Standards Institute Staff and published by . This book was released on 2007-09-28 with total page 26 pages. Available in PDF, EPUB and Kindle. Book excerpt: Food products, Agricultural products, Plant products, Food testing, Chemical analysis and testing, Determination of content, Residues (pesticides), Pesticides, Liquid chromatography, Mass spectrometry


Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites

Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites

Author: Despina Tsipi

Publisher: John Wiley & Sons

Published: 2015-05-12

Total Pages: 288

ISBN-13: 1119070007

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Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries


Book Synopsis Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites by : Despina Tsipi

Download or read book Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites written by Despina Tsipi and published by John Wiley & Sons. This book was released on 2015-05-12 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries


Foods of Plant Origin - Determination of Pesticide Residues Using GC-MS And/or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Clean-Up by Dispersive SPE. QuEChERS-Method

Foods of Plant Origin - Determination of Pesticide Residues Using GC-MS And/or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Clean-Up by Dispersive SPE. QuEChERS-Method

Author: British Standards Institute Staff

Publisher:

Published: 2008-12-31

Total Pages: 84

ISBN-13: 9780580584411

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Food products, Fruits, Vegetables, Cereals, Agricultural products, Chemical analysis and testing, Determination of content, Residues (pesticides), Pesticides, Gas chromatography, Mass spectrometry, Liquid chromatography, Extraction methods of analysis


Book Synopsis Foods of Plant Origin - Determination of Pesticide Residues Using GC-MS And/or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Clean-Up by Dispersive SPE. QuEChERS-Method by : British Standards Institute Staff

Download or read book Foods of Plant Origin - Determination of Pesticide Residues Using GC-MS And/or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Clean-Up by Dispersive SPE. QuEChERS-Method written by British Standards Institute Staff and published by . This book was released on 2008-12-31 with total page 84 pages. Available in PDF, EPUB and Kindle. Book excerpt: Food products, Fruits, Vegetables, Cereals, Agricultural products, Chemical analysis and testing, Determination of content, Residues (pesticides), Pesticides, Gas chromatography, Mass spectrometry, Liquid chromatography, Extraction methods of analysis


Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites

Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites

Author: Despina Tsipi

Publisher: John Wiley & Sons

Published: 2015-05-11

Total Pages: 288

ISBN-13: 111906998X

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Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries


Book Synopsis Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites by : Despina Tsipi

Download or read book Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites written by Despina Tsipi and published by John Wiley & Sons. This book was released on 2015-05-11 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries


Multiresidue Methods for the Analysis of Pesticide Residues in Food

Multiresidue Methods for the Analysis of Pesticide Residues in Food

Author: Horacio Heinzen

Publisher: CRC Press

Published: 2017-10-10

Total Pages: 452

ISBN-13: 1482235102

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In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.


Book Synopsis Multiresidue Methods for the Analysis of Pesticide Residues in Food by : Horacio Heinzen

Download or read book Multiresidue Methods for the Analysis of Pesticide Residues in Food written by Horacio Heinzen and published by CRC Press. This book was released on 2017-10-10 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.


Analysis of Pesticides in Food and Environmental Samples

Analysis of Pesticides in Food and Environmental Samples

Author: Jose L. Tadeo

Publisher: CRC Press

Published: 2008-02-07

Total Pages: 382

ISBN-13: 1420007750

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Developing safety regulations for pesticides used around the world—in excess of 2.5 million tons annually—requires reliable analytical methods for assessing their impact in food and in the environment. Analysis of Pesticides in Food and Environmental Samples presents the most effective techniques for analyzing pesticide residues and other chemical contaminants in foods as well as in soil, water, and air. Renowned Scientists Report New Data and Advances in the Field The book introduces sample preparation, extraction, and analytical methods specific to each sample type, including foods from vegetal and animal origin. Other chapters discuss important aspects of quality assurance and the applicability of hyphenated analytical techniques. In addition to a practical chapter on the use of biosensors and immunoassays for monitoring and gathering exposure data, the book addresses regulatory aspects and presents current data on the levels of pesticides found in food and environmental matrices. Latest Methods Help Scientists Develop Safer, More Effective Pesticides Analysis of Pesticides in Food and Environmental Samples enables scientists to measure and predict the behavior and toxicity of pesticides with a higher degree of accuracy. The methodologies and insight in this timely work will contribute to the development of more effective, less toxic pesticides as well as better safety regulations.


Book Synopsis Analysis of Pesticides in Food and Environmental Samples by : Jose L. Tadeo

Download or read book Analysis of Pesticides in Food and Environmental Samples written by Jose L. Tadeo and published by CRC Press. This book was released on 2008-02-07 with total page 382 pages. Available in PDF, EPUB and Kindle. Book excerpt: Developing safety regulations for pesticides used around the world—in excess of 2.5 million tons annually—requires reliable analytical methods for assessing their impact in food and in the environment. Analysis of Pesticides in Food and Environmental Samples presents the most effective techniques for analyzing pesticide residues and other chemical contaminants in foods as well as in soil, water, and air. Renowned Scientists Report New Data and Advances in the Field The book introduces sample preparation, extraction, and analytical methods specific to each sample type, including foods from vegetal and animal origin. Other chapters discuss important aspects of quality assurance and the applicability of hyphenated analytical techniques. In addition to a practical chapter on the use of biosensors and immunoassays for monitoring and gathering exposure data, the book addresses regulatory aspects and presents current data on the levels of pesticides found in food and environmental matrices. Latest Methods Help Scientists Develop Safer, More Effective Pesticides Analysis of Pesticides in Food and Environmental Samples enables scientists to measure and predict the behavior and toxicity of pesticides with a higher degree of accuracy. The methodologies and insight in this timely work will contribute to the development of more effective, less toxic pesticides as well as better safety regulations.


Food Analysis by HPLC, Second Edition

Food Analysis by HPLC, Second Edition

Author: Leo M.L. Nollet

Publisher: CRC Press

Published: 2000-04-05

Total Pages: 1074

ISBN-13: 9780824784607

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Food Analysis by HPLC, Second Edition presents an exhaustive compilation of analytical methods that belong in the toolbox of every practicing food chemist. Topics covered include biosensors, BMO’s, nanoscale analysis systems, food authenticity, radionuclides concentration, meat factors and meat quality, particle size analysis, and scanning colorimity. It also analyzes peptides, carbohydrates, vitamins, and food additives and contains chapters on alcohols, phenolic compounds, pigments, and residues of growth promoters. Attuned to contemporary food industry concerns, this bestselling classic also features topical coverage of the quantification of genetically modified organisms in food.


Book Synopsis Food Analysis by HPLC, Second Edition by : Leo M.L. Nollet

Download or read book Food Analysis by HPLC, Second Edition written by Leo M.L. Nollet and published by CRC Press. This book was released on 2000-04-05 with total page 1074 pages. Available in PDF, EPUB and Kindle. Book excerpt: Food Analysis by HPLC, Second Edition presents an exhaustive compilation of analytical methods that belong in the toolbox of every practicing food chemist. Topics covered include biosensors, BMO’s, nanoscale analysis systems, food authenticity, radionuclides concentration, meat factors and meat quality, particle size analysis, and scanning colorimity. It also analyzes peptides, carbohydrates, vitamins, and food additives and contains chapters on alcohols, phenolic compounds, pigments, and residues of growth promoters. Attuned to contemporary food industry concerns, this bestselling classic also features topical coverage of the quantification of genetically modified organisms in food.