Chromatography Mass Spectroscopy in Polymer Analysis

Chromatography Mass Spectroscopy in Polymer Analysis

Author: T. R Crompton

Publisher: Smithers Rapra

Published: 2010-12-02

Total Pages: 248

ISBN-13: 184735484X

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The combination of chromatography with mass spectroscopy is a very useful technique which is being increasingly used by polymer chemists to improve existing polymers and to discover new ones with specific physical properties such as thermal stability and retention of properties over a long service life.This technique is extremely powerful for the analysis and characterisation of polymers and is often based on the use of controlled chromatography - mass spectroscopy to measure a polymer's decomposition with techniques such as pyrolysis, followed by chromatography to separate any breakdown product, and, finally, mass spectroscopy, to achieve an unequivocal identification of the pyrolysis products obtained. The detail that can be obtained by such methods includes structure of the polymer backbone, branching, end groups, isomeric detail and fine detail in the structure of copolymers.The first three chapters of the book discuss the various chromatographic and mass spectroscopic techniques now available.Chapters 3-8 cover the complementary methods, based on the combination of mass spectroscopy with various chromatographic techniques such as high-performance liquid chromatography, gas chromatography and supercritical fluid chromatography.Pyrolysis chromatography-mass spectroscopy is a method of studying the structure of polymers which involves subjecting the polymer pyrolysis products to a chromatographic technique to simplify subsequent analysis and, finally mass spectroscopy to identify the pyrolysis products with the possibility of deducing finer details of polymer structure than were previously attainable by classical methods (Chapters 9-11).By providing a thorough up-to-date review of work in this field it is hoped that the book will be of interest to all those engaged in polymer research and development, and polymer users in general.


Book Synopsis Chromatography Mass Spectroscopy in Polymer Analysis by : T. R Crompton

Download or read book Chromatography Mass Spectroscopy in Polymer Analysis written by T. R Crompton and published by Smithers Rapra. This book was released on 2010-12-02 with total page 248 pages. Available in PDF, EPUB and Kindle. Book excerpt: The combination of chromatography with mass spectroscopy is a very useful technique which is being increasingly used by polymer chemists to improve existing polymers and to discover new ones with specific physical properties such as thermal stability and retention of properties over a long service life.This technique is extremely powerful for the analysis and characterisation of polymers and is often based on the use of controlled chromatography - mass spectroscopy to measure a polymer's decomposition with techniques such as pyrolysis, followed by chromatography to separate any breakdown product, and, finally, mass spectroscopy, to achieve an unequivocal identification of the pyrolysis products obtained. The detail that can be obtained by such methods includes structure of the polymer backbone, branching, end groups, isomeric detail and fine detail in the structure of copolymers.The first three chapters of the book discuss the various chromatographic and mass spectroscopic techniques now available.Chapters 3-8 cover the complementary methods, based on the combination of mass spectroscopy with various chromatographic techniques such as high-performance liquid chromatography, gas chromatography and supercritical fluid chromatography.Pyrolysis chromatography-mass spectroscopy is a method of studying the structure of polymers which involves subjecting the polymer pyrolysis products to a chromatographic technique to simplify subsequent analysis and, finally mass spectroscopy to identify the pyrolysis products with the possibility of deducing finer details of polymer structure than were previously attainable by classical methods (Chapters 9-11).By providing a thorough up-to-date review of work in this field it is hoped that the book will be of interest to all those engaged in polymer research and development, and polymer users in general.

Mass Spectrometry in Polymer Chemistry

Mass Spectrometry in Polymer Chemistry

Author: Christopher Barner-Kowollik

Publisher: John Wiley & Sons

Published: 2012-01-27

Total Pages: 501

ISBN-13: 3527641831

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Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.


Book Synopsis Mass Spectrometry in Polymer Chemistry by : Christopher Barner-Kowollik

Download or read book Mass Spectrometry in Polymer Chemistry written by Christopher Barner-Kowollik and published by John Wiley & Sons. This book was released on 2012-01-27 with total page 501 pages. Available in PDF, EPUB and Kindle. Book excerpt: Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.

Mass Spectrometry of Polymers

Mass Spectrometry of Polymers

Author: Giorgio Montaudo

Publisher: CRC Press

Published: 2001-10-29

Total Pages: 601

ISBN-13: 1420037757

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Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results


Book Synopsis Mass Spectrometry of Polymers by : Giorgio Montaudo

Download or read book Mass Spectrometry of Polymers written by Giorgio Montaudo and published by CRC Press. This book was released on 2001-10-29 with total page 601 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results

Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials

Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials

Author: Peter Kusch

Publisher: World Scientific

Published: 2018-10-08

Total Pages: 268

ISBN-13: 1786345773

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The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.


Book Synopsis Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials written by Peter Kusch and published by World Scientific. This book was released on 2018-10-08 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.

Developments in Polymer Analysis and Characterisation

Developments in Polymer Analysis and Characterisation

Author:

Publisher: iSmithers Rapra Publishing

Published: 1999-12

Total Pages: 78

ISBN-13: 9781859571736

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Book Synopsis Developments in Polymer Analysis and Characterisation by :

Download or read book Developments in Polymer Analysis and Characterisation written by and published by iSmithers Rapra Publishing. This book was released on 1999-12 with total page 78 pages. Available in PDF, EPUB and Kindle. Book excerpt:

MALDI Mass Spectrometry for Synthetic Polymer Analysis

MALDI Mass Spectrometry for Synthetic Polymer Analysis

Author: Liang Li

Publisher: John Wiley & Sons

Published: 2009-10-22

Total Pages: 325

ISBN-13: 0470567228

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Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization. It discusses different approaches, including MALDI, ESI, TOF MS, and FT-MS. It provides a guide to developing appropriate sample preparation protocols for different polymers. Complete with examples of applications and experiments, this is an excellent reference for scientists, researchers, graduate students, and others.


Book Synopsis MALDI Mass Spectrometry for Synthetic Polymer Analysis by : Liang Li

Download or read book MALDI Mass Spectrometry for Synthetic Polymer Analysis written by Liang Li and published by John Wiley & Sons. This book was released on 2009-10-22 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization. It discusses different approaches, including MALDI, ESI, TOF MS, and FT-MS. It provides a guide to developing appropriate sample preparation protocols for different polymers. Complete with examples of applications and experiments, this is an excellent reference for scientists, researchers, graduate students, and others.

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)

Author: Peter Kusch

Publisher: World Scientific

Published: 2023-08-28

Total Pages: 383

ISBN-13: 1800613008

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Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.


Book Synopsis Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) written by Peter Kusch and published by World Scientific. This book was released on 2023-08-28 with total page 383 pages. Available in PDF, EPUB and Kindle. Book excerpt: Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.

MALDI-TOF Mass Spectrometry of Synthetic Polymers

MALDI-TOF Mass Spectrometry of Synthetic Polymers

Author: Harald Pasch

Publisher: Springer Science & Business Media

Published: 2013-03-09

Total Pages: 312

ISBN-13: 3662050463

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MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.


Book Synopsis MALDI-TOF Mass Spectrometry of Synthetic Polymers by : Harald Pasch

Download or read book MALDI-TOF Mass Spectrometry of Synthetic Polymers written by Harald Pasch and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 312 pages. Available in PDF, EPUB and Kindle. Book excerpt: MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.

Mass Spectrometry of Polymers – New Techniques

Mass Spectrometry of Polymers – New Techniques

Author: Minna Hakkarainen

Publisher: Springer

Published: 2012-03-24

Total Pages: 212

ISBN-13: 9783642280429

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Emerging Mass Spectrometric Tools for Analysis of Polymers and Polymer Additives, by Nina Aminlashgari and Minna Hakkarainen. Analysis of Polymer Additives and Impurities by Liquid Chromatography/Mass Spectrometry and Capillary Electrophoresis/Mass Spectrometry, by Wolfgang Buchberger and Martin Stiftinger. Direct Insertion Probe Mass Spectrometry of Polymers, by Jale Hacaloglu Mass Spectrometric Characterization of Oligo- and Polysaccharides and Their Derivatives, by Petra Mischnick. Electrospray Ionization-Mass Spectrometry for Molecular Level Understanding of Polymer Degradation, by Minna Hakkarainen.


Book Synopsis Mass Spectrometry of Polymers – New Techniques by : Minna Hakkarainen

Download or read book Mass Spectrometry of Polymers – New Techniques written by Minna Hakkarainen and published by Springer. This book was released on 2012-03-24 with total page 212 pages. Available in PDF, EPUB and Kindle. Book excerpt: Emerging Mass Spectrometric Tools for Analysis of Polymers and Polymer Additives, by Nina Aminlashgari and Minna Hakkarainen. Analysis of Polymer Additives and Impurities by Liquid Chromatography/Mass Spectrometry and Capillary Electrophoresis/Mass Spectrometry, by Wolfgang Buchberger and Martin Stiftinger. Direct Insertion Probe Mass Spectrometry of Polymers, by Jale Hacaloglu Mass Spectrometric Characterization of Oligo- and Polysaccharides and Their Derivatives, by Petra Mischnick. Electrospray Ionization-Mass Spectrometry for Molecular Level Understanding of Polymer Degradation, by Minna Hakkarainen.

Chemical Analysis of Polymers

Chemical Analysis of Polymers

Author: G. Lawson

Publisher: iSmithers Rapra Publishing

Published: 1991-12

Total Pages: 136

ISBN-13: 9780080417424

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Book Synopsis Chemical Analysis of Polymers by : G. Lawson

Download or read book Chemical Analysis of Polymers written by G. Lawson and published by iSmithers Rapra Publishing. This book was released on 1991-12 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt: