NMR Spectroscopy in Food Analysis

NMR Spectroscopy in Food Analysis

Author: Apostolos Spyros

Publisher: Royal Society of Chemistry

Published: 2015-10-20

Total Pages:

ISBN-13: 1782625666

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During the last two decades, the use of NMR spectroscopy for the characterization and analysis of food materials has flourished, and this trend continues to increase today. Currently, there exists no book that fulfils specifically the needs of food scientists that are interested in adding or expanding the use of NMR spectroscopy in their arsenal of food analysis techniques. Current books and monographs are rather addressed to experienced researchers in food analysis providing new information in the field. This book, written by acknowledged experts in the field, fills the gap by offering a day to day NMR guide for the food scientist, affording not only the basic theoretical aspects of NMR spectroscopy, but also practical information on sample preparation, experimental conditions and data analysis. Current developments in the field covered in this book are the availability of solid state NMR experiments such as CP/MAS and more importantly HR-MAS NMR for the analysis of semisolid foods, and the increasing use of chemometrics to analyze NMR data in food metabonomics. Moreover, this book contains an up to date discussion of MRI in food analysis including topics such as food processing and natural changes in food such as ripening. The book is a compact and complete source of information for food scientists who wish to apply methodologies based on NMR spectroscopy in food analysis. It contains information so far scattered in the primary literature, in NMR treatises and food analysis books, in a concise format that makes it appealing to food scientists who have no or minimal experience in magnetic resonance techniques. The inclusion of practical information about NMR instrumentation, experiment setup, acquisition and spectral analysis for the study of different food categories make this book a hands-on manual for food scientists wishing to implement novel NMR spectroscopy-based analytical techniques in their field.


Book Synopsis NMR Spectroscopy in Food Analysis by : Apostolos Spyros

Download or read book NMR Spectroscopy in Food Analysis written by Apostolos Spyros and published by Royal Society of Chemistry. This book was released on 2015-10-20 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: During the last two decades, the use of NMR spectroscopy for the characterization and analysis of food materials has flourished, and this trend continues to increase today. Currently, there exists no book that fulfils specifically the needs of food scientists that are interested in adding or expanding the use of NMR spectroscopy in their arsenal of food analysis techniques. Current books and monographs are rather addressed to experienced researchers in food analysis providing new information in the field. This book, written by acknowledged experts in the field, fills the gap by offering a day to day NMR guide for the food scientist, affording not only the basic theoretical aspects of NMR spectroscopy, but also practical information on sample preparation, experimental conditions and data analysis. Current developments in the field covered in this book are the availability of solid state NMR experiments such as CP/MAS and more importantly HR-MAS NMR for the analysis of semisolid foods, and the increasing use of chemometrics to analyze NMR data in food metabonomics. Moreover, this book contains an up to date discussion of MRI in food analysis including topics such as food processing and natural changes in food such as ripening. The book is a compact and complete source of information for food scientists who wish to apply methodologies based on NMR spectroscopy in food analysis. It contains information so far scattered in the primary literature, in NMR treatises and food analysis books, in a concise format that makes it appealing to food scientists who have no or minimal experience in magnetic resonance techniques. The inclusion of practical information about NMR instrumentation, experiment setup, acquisition and spectral analysis for the study of different food categories make this book a hands-on manual for food scientists wishing to implement novel NMR spectroscopy-based analytical techniques in their field.

Hands on NMR

Hands on NMR

Author: William S. Price

Publisher:

Published: 2021-05-17

Total Pages: 500

ISBN-13: 9781788010887

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Presenting important practical aspects of NMR spectroscopy, this book will be useful for explaining and facilitating the successful set up of a wide variety of NMR experiments. It will enlighten readers with the relevant information on the basic concepts in NMR, how it works, and how to trouble-shoot artefacts that may be encountered. A short introductory chapter on some basic theory and key concepts will precede chapters on more practical aspects e.g. instrumentation, sample preparation, experimentation and data processing. Several practical case experiments covering various fields and including details on the pitfalls, tips and recommendations are presented next. Lastly, detailed chapters on other important practical aspects such as artefacts, spectral prediction, databases and safety are included. Bringing books that present practical NMR up to date, this book fills a gap in the literature and provides a new comprehensive practical NMR book for teaching and research at all levels - graduates, postgraduates, industry and research.


Book Synopsis Hands on NMR by : William S. Price

Download or read book Hands on NMR written by William S. Price and published by . This book was released on 2021-05-17 with total page 500 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presenting important practical aspects of NMR spectroscopy, this book will be useful for explaining and facilitating the successful set up of a wide variety of NMR experiments. It will enlighten readers with the relevant information on the basic concepts in NMR, how it works, and how to trouble-shoot artefacts that may be encountered. A short introductory chapter on some basic theory and key concepts will precede chapters on more practical aspects e.g. instrumentation, sample preparation, experimentation and data processing. Several practical case experiments covering various fields and including details on the pitfalls, tips and recommendations are presented next. Lastly, detailed chapters on other important practical aspects such as artefacts, spectral prediction, databases and safety are included. Bringing books that present practical NMR up to date, this book fills a gap in the literature and provides a new comprehensive practical NMR book for teaching and research at all levels - graduates, postgraduates, industry and research.

Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

Author: John S. Harwood

Publisher: Academic Press

Published: 2015-10-28

Total Pages: 136

ISBN-13: 0128007192

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Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009). Written by experts in solution-state NMR spectroscopy Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer Includes detailed appendices and sample questions for lab reports


Book Synopsis Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers by : John S. Harwood

Download or read book Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers written by John S. Harwood and published by Academic Press. This book was released on 2015-10-28 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt: Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009). Written by experts in solution-state NMR spectroscopy Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer Includes detailed appendices and sample questions for lab reports

NMR Spectroscopy of Polymers

NMR Spectroscopy of Polymers

Author: Tatsuki Kitayama

Publisher: Springer Science & Business Media

Published: 2013-03-09

Total Pages: 231

ISBN-13: 3662089823

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Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.


Book Synopsis NMR Spectroscopy of Polymers by : Tatsuki Kitayama

Download or read book NMR Spectroscopy of Polymers written by Tatsuki Kitayama and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 231 pages. Available in PDF, EPUB and Kindle. Book excerpt: Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.

NMR Spectroscopy Explained

NMR Spectroscopy Explained

Author: Neil E. Jacobsen

Publisher: John Wiley & Sons

Published: 2007-09-10

Total Pages: 640

ISBN-13: 0470173343

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NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.


Book Synopsis NMR Spectroscopy Explained by : Neil E. Jacobsen

Download or read book NMR Spectroscopy Explained written by Neil E. Jacobsen and published by John Wiley & Sons. This book was released on 2007-09-10 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.

Essential Practical NMR for Organic Chemistry

Essential Practical NMR for Organic Chemistry

Author: S. A. Richards

Publisher: John Wiley & Sons

Published: 2023-05-01

Total Pages: 293

ISBN-13: 1119844800

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A hands-on resource advocating an ordered approach to gathering and interpreting NMR data The second edition of Essential Practical NMR for Organic Chemistry delivers a pragmatic and accessible text demonstrating an ordered approach to gathering and interpreting NMR data. In this informal guide, you’ll learn to make sense of the high density of NMR information through the authors’ problem-solving strategies and interpretations. The book also discusses critical aspects of NMR theory, as well as data acquisition and processing strategy. It explains the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation and includes a brand-new chapter on Nitrogen-15 NMR. Readers will also find: Strategies for preparing a sample, spectrum acquisition, processing, and interpreting your spectrum Fulsome discussions of Carbon-13 NMR spectroscopy Practical treatments of quantification, safety procedures, and relevant software An ideal handbook for anyone involved in using NMR to solve structural problems, this latest edition of Essential Practical NMR for Organic Chemistry will be particularly useful for chemists running and looking at their own NMR spectra, as well as those who work in small molecule NMR. It will also earn a place in the libraries of undergraduate and post-graduate organic chemistry students.


Book Synopsis Essential Practical NMR for Organic Chemistry by : S. A. Richards

Download or read book Essential Practical NMR for Organic Chemistry written by S. A. Richards and published by John Wiley & Sons. This book was released on 2023-05-01 with total page 293 pages. Available in PDF, EPUB and Kindle. Book excerpt: A hands-on resource advocating an ordered approach to gathering and interpreting NMR data The second edition of Essential Practical NMR for Organic Chemistry delivers a pragmatic and accessible text demonstrating an ordered approach to gathering and interpreting NMR data. In this informal guide, you’ll learn to make sense of the high density of NMR information through the authors’ problem-solving strategies and interpretations. The book also discusses critical aspects of NMR theory, as well as data acquisition and processing strategy. It explains the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation and includes a brand-new chapter on Nitrogen-15 NMR. Readers will also find: Strategies for preparing a sample, spectrum acquisition, processing, and interpreting your spectrum Fulsome discussions of Carbon-13 NMR spectroscopy Practical treatments of quantification, safety procedures, and relevant software An ideal handbook for anyone involved in using NMR to solve structural problems, this latest edition of Essential Practical NMR for Organic Chemistry will be particularly useful for chemists running and looking at their own NMR spectra, as well as those who work in small molecule NMR. It will also earn a place in the libraries of undergraduate and post-graduate organic chemistry students.

Fundamentals of Protein NMR Spectroscopy

Fundamentals of Protein NMR Spectroscopy

Author: Gordon S. Rule

Publisher: Springer Science & Business Media

Published: 2006-02-16

Total Pages: 543

ISBN-13: 1402035004

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NMR spectroscopy has proven to be a powerful technique to study the structure and dynamics of biological macromolecules. Fundamentals of Protein NMR Spectroscopy is a comprehensive textbook that guides the reader from a basic understanding of the phenomenological properties of magnetic resonance to the application and interpretation of modern multi-dimensional NMR experiments on 15N/13C-labeled proteins. Beginning with elementary quantum mechanics, a set of practical rules is presented and used to describe many commonly employed multi-dimensional, multi-nuclear NMR pulse sequences. A modular analysis of NMR pulse sequence building blocks also provides a basis for understanding and developing novel pulse programs. This text not only covers topics from chemical shift assignment to protein structure refinement, as well as the analysis of protein dynamics and chemical kinetics, but also provides a practical guide to many aspects of modern spectrometer hardware, sample preparation, experimental set-up, and data processing. End of chapter exercises are included to emphasize important concepts. Fundamentals of Protein NMR Spectroscopy not only offer students a systematic, in-depth, understanding of modern NMR spectroscopy and its application to biomolecular systems, but will also be a useful reference for the experienced investigator.


Book Synopsis Fundamentals of Protein NMR Spectroscopy by : Gordon S. Rule

Download or read book Fundamentals of Protein NMR Spectroscopy written by Gordon S. Rule and published by Springer Science & Business Media. This book was released on 2006-02-16 with total page 543 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy has proven to be a powerful technique to study the structure and dynamics of biological macromolecules. Fundamentals of Protein NMR Spectroscopy is a comprehensive textbook that guides the reader from a basic understanding of the phenomenological properties of magnetic resonance to the application and interpretation of modern multi-dimensional NMR experiments on 15N/13C-labeled proteins. Beginning with elementary quantum mechanics, a set of practical rules is presented and used to describe many commonly employed multi-dimensional, multi-nuclear NMR pulse sequences. A modular analysis of NMR pulse sequence building blocks also provides a basis for understanding and developing novel pulse programs. This text not only covers topics from chemical shift assignment to protein structure refinement, as well as the analysis of protein dynamics and chemical kinetics, but also provides a practical guide to many aspects of modern spectrometer hardware, sample preparation, experimental set-up, and data processing. End of chapter exercises are included to emphasize important concepts. Fundamentals of Protein NMR Spectroscopy not only offer students a systematic, in-depth, understanding of modern NMR spectroscopy and its application to biomolecular systems, but will also be a useful reference for the experienced investigator.

Modern NMR Techniques for Chemistry Research

Modern NMR Techniques for Chemistry Research

Author: A.E. Derome

Publisher: Elsevier

Published: 2013-10-22

Total Pages: 299

ISBN-13: 1483286428

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Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.


Book Synopsis Modern NMR Techniques for Chemistry Research by : A.E. Derome

Download or read book Modern NMR Techniques for Chemistry Research written by A.E. Derome and published by Elsevier. This book was released on 2013-10-22 with total page 299 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.

Fast 2D Solution-state NMR

Fast 2D Solution-state NMR

Author: Dr Jean-Nicolas Dumez

Publisher: Royal Society of Chemistry

Published: 2023-05-17

Total Pages: 560

ISBN-13: 183916400X

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Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.


Book Synopsis Fast 2D Solution-state NMR by : Dr Jean-Nicolas Dumez

Download or read book Fast 2D Solution-state NMR written by Dr Jean-Nicolas Dumez and published by Royal Society of Chemistry. This book was released on 2023-05-17 with total page 560 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.

NMR Data Interpretation Explained

NMR Data Interpretation Explained

Author: Neil E. Jacobsen

Publisher: John Wiley & Sons

Published: 2016-10-21

Total Pages: 648

ISBN-13: 1119047145

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Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings


Book Synopsis NMR Data Interpretation Explained by : Neil E. Jacobsen

Download or read book NMR Data Interpretation Explained written by Neil E. Jacobsen and published by John Wiley & Sons. This book was released on 2016-10-21 with total page 648 pages. Available in PDF, EPUB and Kindle. Book excerpt: Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings