Research Techniques for High Pressure and High Temperature

Research Techniques for High Pressure and High Temperature

Author: G. C. Ulmer

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 370

ISBN-13: 3642880975

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Within the last two decades, the experimental technology for the study of high temperature solid-vapor and liquid-vapor equilibria has mushroomed so fast that· both academic and industrial research ers desirous of working in this field -- be they physical chemists, metallurgists, ceramists, petrologists, crystal chemists, or mem bers of any of the several branches of materials science -- find themselves in the situation that in order to learn the art of the latest techniques, a period of apprenticeship or residency needs be spent at an institution or laboratory currently engaged in this type of solid-vapor or liquid-vapor research. The tech niques for control of the vapor phase at total pressures of one atmosphere or greater have not been well defined in the literature. Therefore, the purpose of this volume will be to serve as a labora tory manual for the control, calibration, and measurement of high temperature-high pressure equilibria. The avowed aims of this treatment of experimental techniques are: (1) to give, in terms understandable at the graduate student level, the laboratory procedures necessary to the design and utilization of good experimental technique, (2) to list the limitations, dangers, and technical pitfalls inherent or intrinsic to the described techniques, (3) to give theory and specific data only where they are essential to the experimental design, (4) to give with each chapter references that are extensive enough to serve as a bibliography of the state-of-the-art of technique development within the last decade.


Book Synopsis Research Techniques for High Pressure and High Temperature by : G. C. Ulmer

Download or read book Research Techniques for High Pressure and High Temperature written by G. C. Ulmer and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: Within the last two decades, the experimental technology for the study of high temperature solid-vapor and liquid-vapor equilibria has mushroomed so fast that· both academic and industrial research ers desirous of working in this field -- be they physical chemists, metallurgists, ceramists, petrologists, crystal chemists, or mem bers of any of the several branches of materials science -- find themselves in the situation that in order to learn the art of the latest techniques, a period of apprenticeship or residency needs be spent at an institution or laboratory currently engaged in this type of solid-vapor or liquid-vapor research. The tech niques for control of the vapor phase at total pressures of one atmosphere or greater have not been well defined in the literature. Therefore, the purpose of this volume will be to serve as a labora tory manual for the control, calibration, and measurement of high temperature-high pressure equilibria. The avowed aims of this treatment of experimental techniques are: (1) to give, in terms understandable at the graduate student level, the laboratory procedures necessary to the design and utilization of good experimental technique, (2) to list the limitations, dangers, and technical pitfalls inherent or intrinsic to the described techniques, (3) to give theory and specific data only where they are essential to the experimental design, (4) to give with each chapter references that are extensive enough to serve as a bibliography of the state-of-the-art of technique development within the last decade.

Research Techniques for High Pressure and High Temperature

Research Techniques for High Pressure and High Temperature

Author: G C Ulmer

Publisher:

Published: 1971-01-01

Total Pages: 382

ISBN-13: 9783642880988

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Book Synopsis Research Techniques for High Pressure and High Temperature by : G C Ulmer

Download or read book Research Techniques for High Pressure and High Temperature written by G C Ulmer and published by . This book was released on 1971-01-01 with total page 382 pages. Available in PDF, EPUB and Kindle. Book excerpt:

High-Temperature and High Pressure Crystal Chemistry

High-Temperature and High Pressure Crystal Chemistry

Author: Robert M. Hazen

Publisher: Walter de Gruyter GmbH & Co KG

Published: 2018-12-17

Total Pages: 604

ISBN-13: 1501508709

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Volume 41 of Reviews in Mineralogy and Geochemistry introduces to the field of high-temperature and high-pressure crystal chemistry, both as a guide to the dramatically improved techniques and as a summary of the voluminous crystal chemical literature on minerals at high temperature and pressure. The three parts of the book introduces crystal chemical considerations of special relevance to non-ambient crystallographic studies, reviews the temperature- and pressure-variation of structures in major mineral groups and presents experimental techniques for high-temperature and high-pressure studies of single crystals and polycrystalline samples as well as special considerations relating to diffractometry on samples at non-ambient conditions.


Book Synopsis High-Temperature and High Pressure Crystal Chemistry by : Robert M. Hazen

Download or read book High-Temperature and High Pressure Crystal Chemistry written by Robert M. Hazen and published by Walter de Gruyter GmbH & Co KG. This book was released on 2018-12-17 with total page 604 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volume 41 of Reviews in Mineralogy and Geochemistry introduces to the field of high-temperature and high-pressure crystal chemistry, both as a guide to the dramatically improved techniques and as a summary of the voluminous crystal chemical literature on minerals at high temperature and pressure. The three parts of the book introduces crystal chemical considerations of special relevance to non-ambient crystallographic studies, reviews the temperature- and pressure-variation of structures in major mineral groups and presents experimental techniques for high-temperature and high-pressure studies of single crystals and polycrystalline samples as well as special considerations relating to diffractometry on samples at non-ambient conditions.

Experimental Techniques in High Pressure Research

Experimental Techniques in High Pressure Research

Author: W. F. Sherman

Publisher:

Published: 1987

Total Pages: 496

ISBN-13:

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This book is divided into two sections - the first dealing with the components that work up the high pressure system and the second with the experiments that may be performed with high pressure equipment of relevance to a wide range of disciplines.


Book Synopsis Experimental Techniques in High Pressure Research by : W. F. Sherman

Download or read book Experimental Techniques in High Pressure Research written by W. F. Sherman and published by . This book was released on 1987 with total page 496 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is divided into two sections - the first dealing with the components that work up the high pressure system and the second with the experiments that may be performed with high pressure equipment of relevance to a wide range of disciplines.

Cryotechniques in Biological Electron Microscopy

Cryotechniques in Biological Electron Microscopy

Author: Rudolf A. Steinbrecht

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 308

ISBN-13: 3642728154

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To preserve tissue by freezing is an ancient concept going back pre sumably to the practice of ice-age hunters. At first glance, it seems as simple as it is attractive: the dynamics of life are frozen in, nothing is added and nothing withdrawn except thermal energy. Thus, the result should be more life-like than after poisoning, tan ning and drying a living cell as we may rudely call the conventional preparation of specimens for electron microscopy. Countless mishaps, however, have taught electron microscopists that cryotechniques too are neither simple nor necessarily more life-like in their outcome. Not too long ago, experts in cryotechniques strictly denied that a cell could truly be vitrified, i.e. that all the solutes and macro molecules could be fixed within non-crystalline, glass-like solid water without the dramatic shifts and segregation effects caused by crystallization. We now know that vitrification is indeed pos sible. Growing insight into the fundamentals of the physics of water and ice, as well as increasing experience of how to cool cells rapidly enough have enlivened the interest in cryofixation and pro duced a wealth of successful applications.


Book Synopsis Cryotechniques in Biological Electron Microscopy by : Rudolf A. Steinbrecht

Download or read book Cryotechniques in Biological Electron Microscopy written by Rudolf A. Steinbrecht and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 308 pages. Available in PDF, EPUB and Kindle. Book excerpt: To preserve tissue by freezing is an ancient concept going back pre sumably to the practice of ice-age hunters. At first glance, it seems as simple as it is attractive: the dynamics of life are frozen in, nothing is added and nothing withdrawn except thermal energy. Thus, the result should be more life-like than after poisoning, tan ning and drying a living cell as we may rudely call the conventional preparation of specimens for electron microscopy. Countless mishaps, however, have taught electron microscopists that cryotechniques too are neither simple nor necessarily more life-like in their outcome. Not too long ago, experts in cryotechniques strictly denied that a cell could truly be vitrified, i.e. that all the solutes and macro molecules could be fixed within non-crystalline, glass-like solid water without the dramatic shifts and segregation effects caused by crystallization. We now know that vitrification is indeed pos sible. Growing insight into the fundamentals of the physics of water and ice, as well as increasing experience of how to cool cells rapidly enough have enlivened the interest in cryofixation and pro duced a wealth of successful applications.

Equations of State for Solids at High Pressures and Temperatures

Equations of State for Solids at High Pressures and Temperatures

Author: V. N. Zharkov

Publisher: Springer Science & Business Media

Published: 2013-11-09

Total Pages: 265

ISBN-13: 147571517X

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We started our work on theoretical methods in the phys ics of high pressures (in connec tion with geophysical applications) in 1956, and we immediately encountered many problems. Naturally, we searched the published Iiterature for solutions to these problems but whenever we failed to find a solution or when the solution did not satisfy us, we attempted to solve the problern ourselves. We realized that other investigators working in the physics of high pres sures would probably encounter the same problems and doubts. Therefore, we decided to write this book in order to save our colleagues time and effort. Apart from the descriptions of ex perimental methods, the book deals only with those problems which we encountered in our own work. Allproblems in high-pressure physics have, at present, only approximate solutions, which are very rough. Therefore, it is not surprising that different investigators approach the same problems in different ways. Our approach does not prejudge the issue and we are fully aware that there are other points of view. Our aim was always to solve a glven problern on a physical basis. For example, the concept of the Grüneisenparameter needs further develop ment but it is based on reliable physical ideas. On the other hand, Simon's equation for the melting curve has, in our opinion, no clear physical basis and is purely empirical. Equations of this type are useful in systematic presentation of the experimental material but they are un suitable for any major extrapolation.


Book Synopsis Equations of State for Solids at High Pressures and Temperatures by : V. N. Zharkov

Download or read book Equations of State for Solids at High Pressures and Temperatures written by V. N. Zharkov and published by Springer Science & Business Media. This book was released on 2013-11-09 with total page 265 pages. Available in PDF, EPUB and Kindle. Book excerpt: We started our work on theoretical methods in the phys ics of high pressures (in connec tion with geophysical applications) in 1956, and we immediately encountered many problems. Naturally, we searched the published Iiterature for solutions to these problems but whenever we failed to find a solution or when the solution did not satisfy us, we attempted to solve the problern ourselves. We realized that other investigators working in the physics of high pres sures would probably encounter the same problems and doubts. Therefore, we decided to write this book in order to save our colleagues time and effort. Apart from the descriptions of ex perimental methods, the book deals only with those problems which we encountered in our own work. Allproblems in high-pressure physics have, at present, only approximate solutions, which are very rough. Therefore, it is not surprising that different investigators approach the same problems in different ways. Our approach does not prejudge the issue and we are fully aware that there are other points of view. Our aim was always to solve a glven problern on a physical basis. For example, the concept of the Grüneisenparameter needs further develop ment but it is based on reliable physical ideas. On the other hand, Simon's equation for the melting curve has, in our opinion, no clear physical basis and is purely empirical. Equations of this type are useful in systematic presentation of the experimental material but they are un suitable for any major extrapolation.

High Pressure Processing of Food

High Pressure Processing of Food

Author: V.M. Balasubramaniam

Publisher: Springer

Published: 2016-01-28

Total Pages: 758

ISBN-13: 1493932349

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High pressure processing technology has been adopted worldwide at the industrial level to preserve a wide variety of food products without using heat or chemical preservatives. High Pressure Processing: Technology Principles and Applications will review the basic technology principles and process parameters that govern microbial safety and product quality, an essential requirement for industrial application. This book will be of interest to scientists in the food industry, in particular to those involved in the processing of products such as meat, fish, fruits, and vegetables. The book will be equally important to food microbiologists and processing specialists in both the government and food industry. Moreover, it will be a valuable reference for authorities involved in the import and export of high pressure treated food products. Finally, this update on the science and technology of high pressure processing will be helpful to all academic, industrial, local, and state educators in their educational efforts, as well as a great resource for graduate students interested in learning about state-of-the-art technology in food engineering.


Book Synopsis High Pressure Processing of Food by : V.M. Balasubramaniam

Download or read book High Pressure Processing of Food written by V.M. Balasubramaniam and published by Springer. This book was released on 2016-01-28 with total page 758 pages. Available in PDF, EPUB and Kindle. Book excerpt: High pressure processing technology has been adopted worldwide at the industrial level to preserve a wide variety of food products without using heat or chemical preservatives. High Pressure Processing: Technology Principles and Applications will review the basic technology principles and process parameters that govern microbial safety and product quality, an essential requirement for industrial application. This book will be of interest to scientists in the food industry, in particular to those involved in the processing of products such as meat, fish, fruits, and vegetables. The book will be equally important to food microbiologists and processing specialists in both the government and food industry. Moreover, it will be a valuable reference for authorities involved in the import and export of high pressure treated food products. Finally, this update on the science and technology of high pressure processing will be helpful to all academic, industrial, local, and state educators in their educational efforts, as well as a great resource for graduate students interested in learning about state-of-the-art technology in food engineering.

Residual Stress, Thermomechanics & Infrared Imaging, Hybrid Techniques and Inverse Problems, Volume 9

Residual Stress, Thermomechanics & Infrared Imaging, Hybrid Techniques and Inverse Problems, Volume 9

Author: Sven Bossuyt

Publisher: Springer

Published: 2015-10-29

Total Pages: 364

ISBN-13: 3319217658

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Residual Stress, Thermomechanics& Infrared Imaging, Hybrid Techniques and Inverse Problems, Volume 9 of the Proceedings of the 2015SEM Annual Conference & Exposition on Experimental and Applied Mechanics, the ninth volume of nine from the Conference, brings together contributions to this important area of research and engineering. The collection presents early findings and case studies on a wide range of areas, including: Inverse Methods Inverse Methods in Plasticity Varying Length Scales Harsh Environments Opto-Acoustical Methods Hybrid Experimental Residual Stress Modelling and Advances in Measurements Thermomechanics General Material Response Infrared Imaging


Book Synopsis Residual Stress, Thermomechanics & Infrared Imaging, Hybrid Techniques and Inverse Problems, Volume 9 by : Sven Bossuyt

Download or read book Residual Stress, Thermomechanics & Infrared Imaging, Hybrid Techniques and Inverse Problems, Volume 9 written by Sven Bossuyt and published by Springer. This book was released on 2015-10-29 with total page 364 pages. Available in PDF, EPUB and Kindle. Book excerpt: Residual Stress, Thermomechanics& Infrared Imaging, Hybrid Techniques and Inverse Problems, Volume 9 of the Proceedings of the 2015SEM Annual Conference & Exposition on Experimental and Applied Mechanics, the ninth volume of nine from the Conference, brings together contributions to this important area of research and engineering. The collection presents early findings and case studies on a wide range of areas, including: Inverse Methods Inverse Methods in Plasticity Varying Length Scales Harsh Environments Opto-Acoustical Methods Hybrid Experimental Residual Stress Modelling and Advances in Measurements Thermomechanics General Material Response Infrared Imaging

Carbon at High Temperatures

Carbon at High Temperatures

Author: Alexander Savvatimskiy

Publisher: Springer

Published: 2015-09-07

Total Pages: 257

ISBN-13: 3319213504

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This book deals with the properties and behavior of carbon at high temperatures. It presents new methods and new ways to obtain the liquid phase of carbon. Melting of graphite and the properties of liquid carbon are presented under stationary heat and pulse methods. Metal like properties of molten graphite at high initial density are indicated. A new possible transition of liquid carbon from metal to nonmetal behavior much above the melting point is mentioned. Methodical questions of pulse heating, in particular the role of pinch-pressure in receiving a liquid state of carbon, are discussed. The reader finds evidence about the necessity of applying high pressure (higher than 100 bar) to melt graphite (melting temperature 4800±100 K). The reader can verify the advantage of volume pulse electrical heating before surface laser heating to study the physical properties of carbon, including enthalpy, heat capacity, electrical resistivity and temperature. The advantages of fast heating of graphite by pulsed electric current during a few microseconds are shown. The data obtained for the heat capacity of liquid carbon under constant pressure and constant volume were used to estimate the behavior at temperatures much higher 5000 K.


Book Synopsis Carbon at High Temperatures by : Alexander Savvatimskiy

Download or read book Carbon at High Temperatures written by Alexander Savvatimskiy and published by Springer. This book was released on 2015-09-07 with total page 257 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book deals with the properties and behavior of carbon at high temperatures. It presents new methods and new ways to obtain the liquid phase of carbon. Melting of graphite and the properties of liquid carbon are presented under stationary heat and pulse methods. Metal like properties of molten graphite at high initial density are indicated. A new possible transition of liquid carbon from metal to nonmetal behavior much above the melting point is mentioned. Methodical questions of pulse heating, in particular the role of pinch-pressure in receiving a liquid state of carbon, are discussed. The reader finds evidence about the necessity of applying high pressure (higher than 100 bar) to melt graphite (melting temperature 4800±100 K). The reader can verify the advantage of volume pulse electrical heating before surface laser heating to study the physical properties of carbon, including enthalpy, heat capacity, electrical resistivity and temperature. The advantages of fast heating of graphite by pulsed electric current during a few microseconds are shown. The data obtained for the heat capacity of liquid carbon under constant pressure and constant volume were used to estimate the behavior at temperatures much higher 5000 K.

High Temperature Experiments in Chemistry and Materials Science

High Temperature Experiments in Chemistry and Materials Science

Author: Ketil Motzfeldt

Publisher: John Wiley & Sons

Published: 2012-12-04

Total Pages: 364

ISBN-13: 1118457781

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Cutting edge high temperature materials include high temperature superconductors, solid oxide fuel cells, thermoelectric materials and ultrahigh temperature construction materials (including metals, cermets and ceramics) and have applications in key areas such as energy, transportation and space technologies. This book introduces the concepts which underpin research into these critical materials including thermodynamics, kinetics and various physical, chemical and modelling techniques with a focus on practical “how to” methods and covers: Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances With highly detailed instrument illustrations and an emphasis on the control and measurement of the fundamental properties of temperature, pressure and mass, High Temperature Experiments in Chemistry and Materials Science provides a practical reference on high temperature measurements, for researchers, advanced students and those working in academic or industrial laboratories. Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances


Book Synopsis High Temperature Experiments in Chemistry and Materials Science by : Ketil Motzfeldt

Download or read book High Temperature Experiments in Chemistry and Materials Science written by Ketil Motzfeldt and published by John Wiley & Sons. This book was released on 2012-12-04 with total page 364 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cutting edge high temperature materials include high temperature superconductors, solid oxide fuel cells, thermoelectric materials and ultrahigh temperature construction materials (including metals, cermets and ceramics) and have applications in key areas such as energy, transportation and space technologies. This book introduces the concepts which underpin research into these critical materials including thermodynamics, kinetics and various physical, chemical and modelling techniques with a focus on practical “how to” methods and covers: Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances With highly detailed instrument illustrations and an emphasis on the control and measurement of the fundamental properties of temperature, pressure and mass, High Temperature Experiments in Chemistry and Materials Science provides a practical reference on high temperature measurements, for researchers, advanced students and those working in academic or industrial laboratories. Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances