Solidification of Containerless Undercooled Melts

Solidification of Containerless Undercooled Melts

Author: Dieter M. Herlach

Publisher: John Wiley & Sons

Published: 2012-05-21

Total Pages: 569

ISBN-13: 3527647929

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All metallic materials are prepared from the liquid state as their parent phase. Solidification is therefore one of the most important phase transformation in daily human life. Solidification is the transition from liquid to solid state of matter. The conditions under which material is transformed determines the physical and chemical properties of the as-solidified body. The processes involved, like nucleation and crystal growth, are governed by heat and mass transport. Convection and undercooling provide additional processing parameters to tune the solidification process and to control solid material performance from the very beginning of the production chain. To develop a predictive capability for efficient materials production the processes involved in solidification have to be understood in detail. This book provides a comprehensive overview of the solidification of metallic melts processed and undercooled in a containerless manner by drop tube, electromagnetic and electrostatic levitation, and experiments in reduced gravity. The experiments are accompanied by model calculations on the influence of thermodynamic and hydrodynamic conditions that control selection of nucleation mechanisms and modify crystal growth development throughout the solidification process.


Book Synopsis Solidification of Containerless Undercooled Melts by : Dieter M. Herlach

Download or read book Solidification of Containerless Undercooled Melts written by Dieter M. Herlach and published by John Wiley & Sons. This book was released on 2012-05-21 with total page 569 pages. Available in PDF, EPUB and Kindle. Book excerpt: All metallic materials are prepared from the liquid state as their parent phase. Solidification is therefore one of the most important phase transformation in daily human life. Solidification is the transition from liquid to solid state of matter. The conditions under which material is transformed determines the physical and chemical properties of the as-solidified body. The processes involved, like nucleation and crystal growth, are governed by heat and mass transport. Convection and undercooling provide additional processing parameters to tune the solidification process and to control solid material performance from the very beginning of the production chain. To develop a predictive capability for efficient materials production the processes involved in solidification have to be understood in detail. This book provides a comprehensive overview of the solidification of metallic melts processed and undercooled in a containerless manner by drop tube, electromagnetic and electrostatic levitation, and experiments in reduced gravity. The experiments are accompanied by model calculations on the influence of thermodynamic and hydrodynamic conditions that control selection of nucleation mechanisms and modify crystal growth development throughout the solidification process.

Containerless Processing of Undercooled Melts

Containerless Processing of Undercooled Melts

Author: National Aeronautics and Space Administration (NASA)

Publisher: Createspace Independent Publishing Platform

Published: 2018-06-30

Total Pages: 28

ISBN-13: 9781722128074

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The investigation focused on the control of microstructural evolution in Mn-Al, Fe-Ni, Ni-V, and Au-Pb-Sb alloys through the high undercooling levels provided by containerless processing, and provided fundamental new information on the control of nucleation. Solidification analysis was conducted by means of thermal analysis, x-ray diffraction, and metallographic characterization on samples processed in a laboratory scale drop tube system. The Mn-Al alloy system offers a useful model system with the capability of phase separation on an individual particle basis, thus permitting a more complete understanding of the operative kinetics and the key containerless processing variables. This system provided the opportunity of analyzing the nucleation rate as a function of processing conditions and allowed for the quantitative assessment of the relevant processing parameters. These factors are essential in the development of a containerless processing model which has a predictive capability. Similarly, Ni-V is a model system that was used to study duplex partitionless solidification, which is a structure possible only in high under cooling solidification processes. Nucleation kinetics for the competing bcc and fcc phases were studied to determine how this structure can develop and the conditions under which it may occur. The Fe-Ni alloy system was studied to identify microstructural transitions with controlled variations in sample size and composition during containerless solidification. This work was forwarded to develop a microstructure map which delineates regimes of structural evolution and provides a unified analysis of experimental observations. The Au-Pb-Sb system was investigated to characterize the thermodynamic properties of the undercooled liquid phase and to characterize the glass transition under a variety of processing conditions. By analyzing key containerless processing parameters in a ground based drop tube study, a carefully designed flight experiment may b...


Book Synopsis Containerless Processing of Undercooled Melts by : National Aeronautics and Space Administration (NASA)

Download or read book Containerless Processing of Undercooled Melts written by National Aeronautics and Space Administration (NASA) and published by Createspace Independent Publishing Platform. This book was released on 2018-06-30 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt: The investigation focused on the control of microstructural evolution in Mn-Al, Fe-Ni, Ni-V, and Au-Pb-Sb alloys through the high undercooling levels provided by containerless processing, and provided fundamental new information on the control of nucleation. Solidification analysis was conducted by means of thermal analysis, x-ray diffraction, and metallographic characterization on samples processed in a laboratory scale drop tube system. The Mn-Al alloy system offers a useful model system with the capability of phase separation on an individual particle basis, thus permitting a more complete understanding of the operative kinetics and the key containerless processing variables. This system provided the opportunity of analyzing the nucleation rate as a function of processing conditions and allowed for the quantitative assessment of the relevant processing parameters. These factors are essential in the development of a containerless processing model which has a predictive capability. Similarly, Ni-V is a model system that was used to study duplex partitionless solidification, which is a structure possible only in high under cooling solidification processes. Nucleation kinetics for the competing bcc and fcc phases were studied to determine how this structure can develop and the conditions under which it may occur. The Fe-Ni alloy system was studied to identify microstructural transitions with controlled variations in sample size and composition during containerless solidification. This work was forwarded to develop a microstructure map which delineates regimes of structural evolution and provides a unified analysis of experimental observations. The Au-Pb-Sb system was investigated to characterize the thermodynamic properties of the undercooled liquid phase and to characterize the glass transition under a variety of processing conditions. By analyzing key containerless processing parameters in a ground based drop tube study, a carefully designed flight experiment may b...

Metastable Solids from Undercooled Melts

Metastable Solids from Undercooled Melts

Author: D. M. Herlach

Publisher: Pergamon Press

Published: 2007

Total Pages: 432

ISBN-13: 9780080436388

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This book presents the physical concepts and tools to characterize and describe the formation of metastable solids from undercooled melts. Its aim is to facilitate understanding of the development of the science and technology of solidification of melts and to introduce new concepts within this exciting research field in order to fulfil the challenges of the future in the field of undercooled melts. A comprehensive description of the science and applications of the undercooling phenomenon is given. It is composed of several main parts: experimental techniques for undercooling; characterization of the undercooled melt as the first step in rapid solidification; introducing the concepts of modern theories of rapid dendrite and eutectic growth and their comparison with experimental results, and a survey of metastable materials formed from the non-equilibrium state of an undercooled melt. * Showing clear links to possible application of results obtained from basic research * The subject matter is multidisciplinary and will be of interest to material scientists, physicists, physical chemists, mechanical and electrical engineers


Book Synopsis Metastable Solids from Undercooled Melts by : D. M. Herlach

Download or read book Metastable Solids from Undercooled Melts written by D. M. Herlach and published by Pergamon Press. This book was released on 2007 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents the physical concepts and tools to characterize and describe the formation of metastable solids from undercooled melts. Its aim is to facilitate understanding of the development of the science and technology of solidification of melts and to introduce new concepts within this exciting research field in order to fulfil the challenges of the future in the field of undercooled melts. A comprehensive description of the science and applications of the undercooling phenomenon is given. It is composed of several main parts: experimental techniques for undercooling; characterization of the undercooled melt as the first step in rapid solidification; introducing the concepts of modern theories of rapid dendrite and eutectic growth and their comparison with experimental results, and a survey of metastable materials formed from the non-equilibrium state of an undercooled melt. * Showing clear links to possible application of results obtained from basic research * The subject matter is multidisciplinary and will be of interest to material scientists, physicists, physical chemists, mechanical and electrical engineers

Science and Technology of the Undercooled Melt

Science and Technology of the Undercooled Melt

Author: P.R. Sahm

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 296

ISBN-13: 940094456X

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"SCIENCE AND TECHNOLOGY OF '!HE UNDEROLED MELT" This title was chosen as the topical headline of the Advanced Research Workshop (ARW) from March 17 to 22 1985, held at the Castle of Theuern. The usual term "Rapid Solidification" is an overlapping description. Due to the fact that nucleation is so eminently important for the undercooling of a melt and this, in turn, is an important characteristic of rapid solidifi cation, undercooling plays an essential role in "rapid solidification." The undercooled melt has caused an "accelerated evolution" (if not a revolution) in materials science during the last decade. Several rather exciting concepts with interesting potential for novel applications are being pursued presently in various laboratories and companies. They concern not only new processes and ha~ware developments, but also present chal lenging perspectives for ventures, including the founding of new companies; or they promise growth possibilities with established larger and smaller industrial establishments.


Book Synopsis Science and Technology of the Undercooled Melt by : P.R. Sahm

Download or read book Science and Technology of the Undercooled Melt written by P.R. Sahm and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 296 pages. Available in PDF, EPUB and Kindle. Book excerpt: "SCIENCE AND TECHNOLOGY OF '!HE UNDEROLED MELT" This title was chosen as the topical headline of the Advanced Research Workshop (ARW) from March 17 to 22 1985, held at the Castle of Theuern. The usual term "Rapid Solidification" is an overlapping description. Due to the fact that nucleation is so eminently important for the undercooling of a melt and this, in turn, is an important characteristic of rapid solidifi cation, undercooling plays an essential role in "rapid solidification." The undercooled melt has caused an "accelerated evolution" (if not a revolution) in materials science during the last decade. Several rather exciting concepts with interesting potential for novel applications are being pursued presently in various laboratories and companies. They concern not only new processes and ha~ware developments, but also present chal lenging perspectives for ventures, including the founding of new companies; or they promise growth possibilities with established larger and smaller industrial establishments.

Metallurgy in Space

Metallurgy in Space

Author: Hans-Jörg Fecht

Publisher: Springer Nature

Published: 2022-03-31

Total Pages: 564

ISBN-13: 3030897842

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This book presents experimental work conducted on the International Space Station (ISS) in order to characterize metals and alloys in the liquid state. The internationally recognized authors present and discuss experiments performed in microgravity that enabled the study of the relevant volume and surface related properties free of the restrictions of a gravity-based environment. The collection serves also as a handbook of space experiments using electromagnetic levitation techniques. A summary of recent results provides an overview of the wealth of space experiment data, which will ignite further research activities and inspire academics and industrial research departments for their continuous development.


Book Synopsis Metallurgy in Space by : Hans-Jörg Fecht

Download or read book Metallurgy in Space written by Hans-Jörg Fecht and published by Springer Nature. This book was released on 2022-03-31 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents experimental work conducted on the International Space Station (ISS) in order to characterize metals and alloys in the liquid state. The internationally recognized authors present and discuss experiments performed in microgravity that enabled the study of the relevant volume and surface related properties free of the restrictions of a gravity-based environment. The collection serves also as a handbook of space experiments using electromagnetic levitation techniques. A summary of recent results provides an overview of the wealth of space experiment data, which will ignite further research activities and inspire academics and industrial research departments for their continuous development.

Rapid Solidification of Undercooled Melts

Rapid Solidification of Undercooled Melts

Author: Xiaolong Xu

Publisher:

Published: 2018

Total Pages:

ISBN-13:

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Rapid solidification and microstructure evolution of deeply undercooled bulk concentrated Ni-20%at.Cu and Co-20%at.Pd alloys are strictly and systematically evaluated. First, thermodynamics of the undercooled melt is discussed. Consideration is provided for not only the systematic microstructure evolution within a broad undercooling range, but also the dendrite growth mechanism and the rapid solidification characteristics. The dendrite growth in the bulk undercooled melts was captured by a high speed camera. The first kind of grain refinement occurring in the low undercooling regimes was explained by a current grain refinement model. Besides for the dendrite melting mechanism, the stress originating from the solidification contraction and thermal strain in the first mushy zone during rapid solidification could be a main mechanism causing the second kind of grain refinement above the critical undercooling. This internal-stress led to the distortion and breakup of the primary dendrites and was semi-quantitatively described by a corrected stress accumulation model. It was found that the stress induced recrystallization could make the primary microstructures refine substantially after recalescence.


Book Synopsis Rapid Solidification of Undercooled Melts by : Xiaolong Xu

Download or read book Rapid Solidification of Undercooled Melts written by Xiaolong Xu and published by . This book was released on 2018 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Rapid solidification and microstructure evolution of deeply undercooled bulk concentrated Ni-20%at.Cu and Co-20%at.Pd alloys are strictly and systematically evaluated. First, thermodynamics of the undercooled melt is discussed. Consideration is provided for not only the systematic microstructure evolution within a broad undercooling range, but also the dendrite growth mechanism and the rapid solidification characteristics. The dendrite growth in the bulk undercooled melts was captured by a high speed camera. The first kind of grain refinement occurring in the low undercooling regimes was explained by a current grain refinement model. Besides for the dendrite melting mechanism, the stress originating from the solidification contraction and thermal strain in the first mushy zone during rapid solidification could be a main mechanism causing the second kind of grain refinement above the critical undercooling. This internal-stress led to the distortion and breakup of the primary dendrites and was semi-quantitatively described by a corrected stress accumulation model. It was found that the stress induced recrystallization could make the primary microstructures refine substantially after recalescence.

Rapidly Solidified Alloys

Rapidly Solidified Alloys

Author: Liebermann

Publisher: CRC Press

Published: 1993-05-20

Total Pages: 804

ISBN-13: 9780824789510

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This volume details the principles underlying rapid solidification processing, material structure and properties, and their applications. This practical resource presents a manifold approach to both amorphous and crystalline rapidly solidified metallic alloys.;Written by over 30 internationally acclaimed specialists in their respective fields, Rapidly Solidified Alloys: surveys nucleation and growth studies in undercooled melts; examines various processes for the production of rapidly solidified alloys; discusses the compaction of amorphous alloys; describes surface remelting treatments for the rapid solidification of surface layers and the resultant improved workpiece properties; covers the closely related topics of structural relaxation, atomic transport and other thermally induced processes; demonstrates microstructure-property relationships in rapidly quenched crystalline alloy systems and their beneficial effects in applications; and elucidates the basic, engineeering, and applications-oriented magnetic properties of amorphous alloys.;Furnishing more than 2300 literature citations for further study of specific subjects, Rapidly Solidified Alloys is intended for materials, mechanical, product, and civil engineers; metallurgists; magneticians; physicists; physical chemists; and graduate students in these disciplines.


Book Synopsis Rapidly Solidified Alloys by : Liebermann

Download or read book Rapidly Solidified Alloys written by Liebermann and published by CRC Press. This book was released on 1993-05-20 with total page 804 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume details the principles underlying rapid solidification processing, material structure and properties, and their applications. This practical resource presents a manifold approach to both amorphous and crystalline rapidly solidified metallic alloys.;Written by over 30 internationally acclaimed specialists in their respective fields, Rapidly Solidified Alloys: surveys nucleation and growth studies in undercooled melts; examines various processes for the production of rapidly solidified alloys; discusses the compaction of amorphous alloys; describes surface remelting treatments for the rapid solidification of surface layers and the resultant improved workpiece properties; covers the closely related topics of structural relaxation, atomic transport and other thermally induced processes; demonstrates microstructure-property relationships in rapidly quenched crystalline alloy systems and their beneficial effects in applications; and elucidates the basic, engineeering, and applications-oriented magnetic properties of amorphous alloys.;Furnishing more than 2300 literature citations for further study of specific subjects, Rapidly Solidified Alloys is intended for materials, mechanical, product, and civil engineers; metallurgists; magneticians; physicists; physical chemists; and graduate students in these disciplines.

Metastable Solids from Undercooled Melts

Metastable Solids from Undercooled Melts

Author: Dieter Herlach

Publisher: Elsevier

Published: 2006-12-18

Total Pages: 445

ISBN-13: 0080468861

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This book presents the physical concepts and tools to characterize and describe the formation of metastable solids from undercooled melts. Its aim is to facilitate understanding of the development of the science and technology of solidification of melts and to introduce new concepts within this exciting research field in order to fulfil the challenges of the future in the field of undercooled melts. A comprehensive description of the science and applications of the undercooling phenomenon is given. It is composed of several main parts: experimental techniques for undercooling; characterization of the undercooled melt as the first step in rapid solidification; introducing the concepts of modern theories of rapid dendrite and eutectic growth and their comparison with experimental results, and a survey of metastable materials formed from the non-equilibrium state of an undercooled melt. * Showing clear links to possible application of results obtained from basic research * The subject matter is multidisciplinary and will be of interest to material scientists, physicists, physical chemists, mechanical and electrical engineers


Book Synopsis Metastable Solids from Undercooled Melts by : Dieter Herlach

Download or read book Metastable Solids from Undercooled Melts written by Dieter Herlach and published by Elsevier. This book was released on 2006-12-18 with total page 445 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents the physical concepts and tools to characterize and describe the formation of metastable solids from undercooled melts. Its aim is to facilitate understanding of the development of the science and technology of solidification of melts and to introduce new concepts within this exciting research field in order to fulfil the challenges of the future in the field of undercooled melts. A comprehensive description of the science and applications of the undercooling phenomenon is given. It is composed of several main parts: experimental techniques for undercooling; characterization of the undercooled melt as the first step in rapid solidification; introducing the concepts of modern theories of rapid dendrite and eutectic growth and their comparison with experimental results, and a survey of metastable materials formed from the non-equilibrium state of an undercooled melt. * Showing clear links to possible application of results obtained from basic research * The subject matter is multidisciplinary and will be of interest to material scientists, physicists, physical chemists, mechanical and electrical engineers

Solidification Behaviour and Precipitation Phenomena in Undercooled Melts

Solidification Behaviour and Precipitation Phenomena in Undercooled Melts

Author: Octavian Filip

Publisher:

Published: 2003

Total Pages: 103

ISBN-13:

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Book Synopsis Solidification Behaviour and Precipitation Phenomena in Undercooled Melts by : Octavian Filip

Download or read book Solidification Behaviour and Precipitation Phenomena in Undercooled Melts written by Octavian Filip and published by . This book was released on 2003 with total page 103 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Phase Transformations in Multicomponent Melts

Phase Transformations in Multicomponent Melts

Author: Dieter M. Herlach

Publisher: John Wiley & Sons

Published: 2009-06-10

Total Pages: 435

ISBN-13: 3527624058

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Bringing together the concerted efforts of the multicomponent materials community in one decisive reference work, this handbook covers all the important aspects from fundamentals to applications: thermodynamics, microscopic processes, solidification, simulation and modeling. As such, it provides a vital understanding of melt and solidification processes, treating all simulation techniques for continuous and discrete systems, such as molecular dynamics, Monte Carlo, and finite elements calculations.


Book Synopsis Phase Transformations in Multicomponent Melts by : Dieter M. Herlach

Download or read book Phase Transformations in Multicomponent Melts written by Dieter M. Herlach and published by John Wiley & Sons. This book was released on 2009-06-10 with total page 435 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bringing together the concerted efforts of the multicomponent materials community in one decisive reference work, this handbook covers all the important aspects from fundamentals to applications: thermodynamics, microscopic processes, solidification, simulation and modeling. As such, it provides a vital understanding of melt and solidification processes, treating all simulation techniques for continuous and discrete systems, such as molecular dynamics, Monte Carlo, and finite elements calculations.